JCTLM Database: higher-order reference materials, methods and services
Details : C14RMP11 - NCCL ID LC-MS/MS reference measurement procedure for glucose
| Type (acronym) | rmp |
| Type | reference measurement procedure |
| Unique Nomination Number | C14RMP11 |
| Analyte Name | glucose |
| IUPAC IFCC Number | CAS50-99-7 |
| Method capable of Traceability of Analyte to SI or Defined Procedure | SI |
| Applicable Matrices | human serum; fresh, frozen or lyophilized |
| Name | NCCL ID LC-MS/MS reference measurement procedure for glucose |
| Organization that developed Validated Method | National Center for Clinical Laboratories (NCCL) |
| Measurement Techniques Used | Isotope Dilution Mass Spectrometry (IDMS), Liquid Chromatography Mass Spectrometry (LCMS) |
| Quantity | Amount-of-substance fraction |
| From (0) | 1.5 |
| To (0) | 25 |
| Unit (0) | mmol/L |
| From (1) | 0.5 |
| To (1) | 1.5 |
| Unit (1) | % |
| Level of Confidence (%) | 95% |
| Peer Reviewed Publication | Determination of serum glucose by isotope dilution liquid chromatography-tandem mass spectrometry: a candidate reference measurement procedure, Zhang T, et al., Analytical Bioanalytical Chemistry, 2016, 408(26), 7403-7411
|
| Additional Comments | No |
| Hyperlink to Final Report of extent of Equivalence Studies among | IFCC External Quality assessment scheme for Reference Laboratories in Laboratory Medicine (RELA), lab code 18, Results year 2012 and 2014 |
| Analyte Category Name | Metabolites and substrates |
| Non-CCQM Key Comparison Report | Agreement between the ID LC-MS/MS and the ID GC-MS reference measurement procedures for Glucose, Electronic Supplement Material of Analytical Bioanalytical Chemistry 2016 publication. |
| Non-CCQM Key Comparison Report Hyperlink | https://static-content.springer.com/esm/art%3A10.1007%2Fs00216-016-9817-0/MediaObjects/216_2016_9817_MOESM1_ESM.pdf |
| Measurement principle/technique | Isotope dilution mass spectrometry |
| Measurement principle/technique | Liquid chromatography mass spectrometry |