JCTLM Database: higher-order reference materials, methods and services
Details : NRMeth 46 - DGKC reference method for serum cholesterol
| Type (acronym) | rmp |
| Type | reference measurement procedure |
| Unique Nomination Number | NRMeth 46 |
| Analyte Name | total cholesterol |
| IUPAC IFCC Number | CAS57-88-5 |
| Method capable of Traceability of Analyte to SI or Defined Procedure | SI |
| Applicable Matrices | lyophilized, fresh, or frozen human serum or plasma |
| Name | DGKC reference method for serum cholesterol |
| Organization that developed Validated Method | German Society of Clinical Chemistry (DGKC) |
| Measurement Techniques Used | ID/GC/MS |
| Comments 1 | trimethylsilyl derative |
| Comments 2 | Calibrate with SRM 911b, high purity cholesterol |
| Quantity | Amount-of-substance concentration |
| From (0) | 2 |
| To (0) | 10 |
| Unit (0) | mmol/l |
| From (1) | 0.5 |
| To (1) | 1.5 |
| Unit (1) | % |
| Level of Confidence (%) | 95% |
| Peer Reviewed Publication | Siekmann et al., Z. anal. Chem., 1976, 279, 145-146
|
| Review Team Name | metabolites and substrates |
| Analyte Category Name | Metabolites and substrates |
| CCQM Key Comparison Report | Metrologia, 2004, 39, Tech. Suppl., 08001
|
| CCQM Key Comparison Report Hyperlink | http://stacks.iop.org/met/39/08001 |
| Measurement principle/technique | Isotope dilution mass spectrometry |