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Details : NRMeth 49 - DGKC reference method for serum total glycerol
| Type (acronym) | rmp |
|---|---|
| Type | reference measurement procedure |
| Unique Nomination Number | NRMeth 49 |
| Analyte Name | total glycerol |
| IUPAC IFCC Number | total glycerol |
| Method capable of Traceability of Analyte to SI or Defined Procedure | SI |
| Applicable Matrices | lyophilized, fresh, or frozen human serum or plasma |
| Name | DGKC reference method for serum total glycerol |
| Organization that developed Validated Method | German Society of Clinical Chemistry (DGKC) |
| Measurement Techniques Used | ID/GC/MS |
| Comments 1 | trimethylsilyl derative |
| Comments 2 | Calibrate with SRM 1595, high purity glycerol tripalmitate |
| Quantity | Amount-of-substance concentration |
| From (0) | 0.5 |
| To (0) | 11 |
| Unit (0) | mmol/l |
| From (1) | 0.5 |
| To (1) | 1.5 |
| Unit (1) | % |
| Level of Confidence (%) | 95% |
| Peer Reviewed Publication | Siekmann et al., Z.anal. Chem., 1986, 324, 280-281 |
| Comments to be published via JCTLM DB | This reference measurement procedure measures 'total glycerol' in serum, which is the sum of triglycerides, diglycerides, monoglycerides, and free glycerol. |
| Review Team Name | metabolites and substrates |
| Analyte Category Name | Metabolites and substrates |
| Non-CCQM Key Comparison Report | Benchmarked with PTB reference method for serum total glycerol |
| Non-CCQM Key Comparison Report Hyperlink | |
| Non-CCQM Key Comparison Report | for information, contact lothar.siekmann@ukb.uni-bonn.de |
| Non-CCQM Key Comparison Report Hyperlink | |
| Measurement principle/technique | Isotope dilution mass spectrometry |